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X-ray diffraction technique have been using for a long time to understand the characteristics of various materials around the world. So it is important to understand the kinematics and dynamical theory and their applications in different cases. So dynamical theory of x-ray diffraction for both absorption and without absorption is developed and applied to thin, thick and intermediate thick CuZn alloy to obtain the diffraction patterns for both Bragg's and Laue's cases. The famous asymmetric curve is found when absorption is considered; the diffraction curve is symmetrical without absorption. It is found that the intensity increases but FWHM decreases for higher indices. Order-disorder transformation of CuZn binary alloy is also noticed for various temperatures. The atomic scattering factors of different elements are calculated to see the temperature effect. The temperature dependence of reflection lines are computed using Debye and Einstein approximation. Interestingly intensity of reflection lines decreases with the increase of temperature and indices for both cases. This book will be helpful for the student and researchers who want to understand and work on x-ray diffraction.
This volume collects the proceedings of the 23rd International Course of Crystallography, entitled "X-ray and Neutron Dynamical Diffraction, Theory and Applications," which took place in the fascinating setting of Erice in Sicily, Italy. It was run as a NATO Advanced Studies Institute with A. Authier (France) and S. Lagomarsino (Italy) as codirectors, and L. Riva di Sanseverino and P. Spadon (Italy) as local organizers, R. Colella (USA) and B. K. Tanner (UK) being the two other members of the organizing committee. It was attended by about one hundred participants from twenty four different countries. Two basic theories may be used to describe the diffraction of radiation by crystalline matter. The first one, the so-called geometrical, or kinematical theory, is approximate and is applicable to small, highly imperfect crystals. It is used for the determination of crystal structures and describes the diffraction of powders and polycrystalline materials. The other one, the so-called dynamical theory, is applicable to perfect or nearly perfect crystals. For that reason, dynamical diffraction of X-rays and neutrons constitutes the theoretical basis of a great variety of applications such as: • the techniques used for the characterization of nearly perfect high technology materials, semiconductors, piezoelectric, electrooptic, ferroelectric, magnetic crystals, • the X-ray optical devices used in all modem applications of Synchrotron Radiation (EXAFS, High Resolution X-ray Diffractometry, magnetic and nuclear resonant scattering, topography, etc. ), and • X-ray and neutron interferometry.
The proposed nonstandard diffraction theory is constructed directly from the Maxwell equations for the crystalline medium in the X-ray wavelength range. Analysis of Maxwell?s equations for dynamic diffraction is possible using the method of multiple scales which is modified to the vector character of the problem. In this case, the small parameter of the expansion is the Fourier component of the polarizability of the crystal. The second-order wave equation is analyzed without any assumptions about the possibility of the interaction between the refracted and scattered waves which automatically leads to the dynamic character of the scattering. The unified consideration of different geometrical schemes of diffraction including grazing geometry is possible. This is due to the construction of a unified wave field in the crystal and obtaining the field amplitudes according to the boundary conditions. The proposed theory allows generalization to the case of an imperfect crystal. Thus, a unified approach to account for deformations and other crystal structure disturbances in all diffraction schemes is implemented. The determination of a unified wave field without separation of the refracted and scattered waves is of the greatest importance in the analysis of secondary processes.