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This report presents a cost analysis of Ammonium Chloride production from ammonia and hydrogen chloride. The process examined is a typical solution neutralization process. In the process, hydrogen chloride reacts with ammonia, producing Ammonium Chloride crystals, which are centrifuged and dried. The mother liquor from the centrifuge is recycled back to the reactors. This report was developed based essentially on the following reference(s): Keywords: Hydrochloric Acid, Sal Ammoniac, Azane
This report presents a cost analysis of Methyl Chloride production from methanol and hydrogen chloride The process examined is a typical catalytic vapor phase process. In this process, methanol and anhydrous HCl are combined in vapor phase and passed through a catalyst bed. Reactor vapor outlet is quenched, dried by sulfuric acid scrubbing and then purified to generate high-purity Methyl Chloride. This report was developed based essentially on the following reference(s): (1) "Chloromethanes", Ullmann's Encyclopedia of Industrial Chemistry, 2012; (2) Handbook of Industrial Chemistry and Biotechnology, 2012 Keywords: Chloromethane, R-40, HCC-40, chlorosilanes production
This report presents a cost analysis of a typical Titanium Butoxide production process from butyl alcohol, titanium tetrachloride, and ammonia. In the process, titanium tetrachloride and butyl alcohol react producing titanium butoxide and chlorine. Ammonia is added to recover the chlorine in the form of ammonium chloride. This report was developed based essentially on the following reference(s): Keywords: Butyl Titanate, Tetra Butyl Titanate
This report presents a cost analysis of Precipitated Calcium Carbonate (PCC) production from limestone. In this typical process, limestone is first calcinated. The product reacts with water producing calcium hydroxide, which is further carbonated with carbon dioxide from calcination to produce PCC. This report was developed based essentially on the following reference(s): (1) US Patent 6251356, issued to G. R. International in 2001 (assigned to Pacific Nano Products in 2015) (2) US Patent 3920800, issued to Cyprus Mines Corporation in 1975 Keywords: Calcite, Aragonite, Calcine, Hydrated Lime, Slaked Lime
This report presents a cost analysis of Sodium Cyanide production from metallic sodium, charcoal and ammonia. In this process, molten sodium, ammonia, and charcoal react to form Sodium Cyanide. The product Sodium Cyanide is removed as a liquid and flaked to its final form. This report was developed based essentially on the following reference(s): Keywords: Metallic Sodium Process, NaCN, Molten Sodium
This report presents a cost analysis of Isophorone Diisocyanate (IPDI) production from isophorone and chlorine. The process examined is a typical phosgenation process. In this process, isophorone diamine (IPDA) intermediate is initially obtained from isophorone. Then, IPDA reacts with phosgene to produce IPDI. The phosgene used is generated from chlorine and carbon monoxide in an on-site unit. Hydrogen chloride (HCl) is generated as by-product. This report was developed based essentially on the following reference(s): (1) US Patent 9187412 B2, issued to Evonik Degussa in 2015 (2) US Patent 8884063 B2, issued to BASF SE in 2014 (3) US Patent 8563768, issued to Covestro (fromer Bayer MaterialScience) in 2013 Keywords: Isophorone Diisocyanate, IPDI, Isophorone Diamine, IPDA, Phosgenation
This report presents a cost analysis of Propylene Oxide (PO) production from chemical grade (CG) propylene and chlorine. The process examined is a typical chlorohydrin process. In this process, propylene and chlorine first react to produce propylene chlorohydrin intermediate. Then, the chlorohydrin intermediate is dehydrochlorinated to Propylene Oxide. Dichloropropane is generated as by-product in the process. This report was developed based essentially on the following reference(s): "Propylene Oxide", Ullmann's Encyclopedia of Industrial Chemistry, 7th edition Keywords: Chlorohydrination, Saponification, Calcium Oxide, CaO, Calcium Hydroxide, CHPO
The gold standard in analytical chemistry, Dan Harris’ Quantitative Chemical Analysis provides a sound physical understanding of the principles of analytical chemistry and their applications in the disciplines
This monograph consists of manuscripts submitted by invited speakers who participated in the symposium "Industrial Environmental Chemistry: Waste Minimization in Industrial Processes and Remediation of Hazardous Waste," held March 24-26, 1992, at Texas A&M University. This meeting was the tenth annual international symposium sponsored by the Texas A&M Industry-University Cooperative Chemistry Program (IUCCP). The program was developed by an academic-industrial steering committee consisting of the co-chairmen, Professors Donald T. Sawyer and Arthur E. Martell of the Texas A&M University Chemistry Department, and members appointed by the sponsoring companies: Bernie A. Allen, Jr., Dow Chemical USA; Kirk W. Brown, Texas A&M University; Abraham Clearfield, Texas A&M University; Greg Leyes, Monsanto Company; Jay Warner, Hoechst-Celanese Corporation; Paul M. Zakriski, BF Goodrich Company; and Emile A. Schweikert, Texas A&M University (IUCCP Coordinator). The subject of this conference reflects the interest that has developed in academic institutions and industry for technological solutions to environmental contamination by industrial wastes. Progress is most likely with strategies that minimize waste production from industrial processes. Clearly the key to the protection and preservation of the environment will be through R&D that optimizes chemical processes to minimize or eliminate waste streams. Eleven of the papers are directed to waste minimization. An additional ten papers discuss chemical and biological remediation strategies for hazardous wastes that contaminate soils, sludges, and water.
Analytical methods used in the Geologic Division laboratories of the U.S. Geological Survey for the inorganic chemical analysis of rock and mineral samples.